Pengaruh Perlakuan Panas Karburisasi Austemper pada Baja Laterit Paduan Cr-Mo terhadap Sifat Mekanik dan Struktur Mikro

Satrio Herbirowo, Vinda Puspasari, M. Iqbal Primatama, Hendrik Hendrik, I Nyoman Gede Putrayasa Astawa, Bintang Adjiantoro, Andika Widya Pramono

Abstract


This research was aimed to do heat treatment of austemper carburization and investigate the effect of various cooling media on mechanical properties and microstructure of Cr-Mo alloy lateritic steel. Heat treatment was conducted to austenisation temperature at 950o C for 1 hour and austemper carburization at 400o C for 1 hour. Variation of cooling media included air blowing for 1 hour, water, and furnace cooling for 24 hours. Hardness and impact test were done using Hardness Rockwell and Charpy methods. Microstructure was observed using optical microscope. Fracture surface characterization was using SEM-EDX. The results showed the highest hardness of 65.48 HRC in sample that cooled by air blowing for 1 hour. The microstructure of this sample showed phases of ferrite, pearlite and martensite which causing higher hardness. The highest impact strength of 20 Joule took place in the furnace cooled sample. Characterization of the fracture surface using SEM-EDX showed dimple of ductile fractures.


Penelitian ini bertujuan untuk melakukan proses perlakukan panas karburisasi austemper dan mempelajari pengaruh media pendinginan terhadap sifat mekanik dan struktur mikro baja laterit paduan Cr-Mo. Perlakuan panas yang dilakukan yaitu pemanasan sampel pada temperatur austenisasi (950o C) selama 1 jam dan proses karburisasi austemper dengan media serbuk arang halus pada temperatur 400o C selama 1 jam. Variasi pendinginan yang digunakan yaitu air blowing (semburan udara) selama 1 jam, air dan tungku selama 24 jam. Pengujian kekerasan dilakukan dengan metode Rockwell Hardness dan pengujian impak dilakukan dengan metode charpy. Karakterisasi struktur mikro dilakukan dengan proses metalografi dan mikroskop optik. Karakterisasi permukaan patahan pengujian impak dilakukan dengan SEM-EDX. Hasil penelitian ini menunjukkan nilai kekerasan tertinggi yaitu 65,48 HRC terjadi pada sampel dengan air blowing selama 1 jam. Struktur mikro sampel tersebut menunjukkan adanya fasa ferit, perlit dan martensit yang membuat sampel menjadi keras. Nilai kekuatan impak tertinggi sebesar 20 Joule terjadi pada sampel dengan pendinginan di dalam tungku selama 24 jam. Karakterisasi permukaan patahannya menggunakan SEM-EDX menunjukkan adanya dimple dari patah ulet.



Keywords


baja laterit, austemper, dimple, sifat mekanik dan strukur mikro

Full Text:

PDF

References


R. Subagja, A. B. Prasetyo, and W. M. Sari, “Peningkatan Kadar Nikel dalam Laterit Jenis Limonit dengan Cara Peletasi, Pemanggangan Reduksi dan Pemisahan Magnet Campuran Bijih, Baru bara, dan Na2SO4,” J. Mater. Metal., vol. 2, pp. 103–115, 2016.

H. Basturkcu, M. Achimovičová, M. Kaňuchová, and N. Acarkan, “Mechanochemical pre-treatment of lateritic nickel ore with sulfur followed by atmospheric leaching,” Hydrometallurgy, 2018., doi:10.1016/j.hydromet.2018.08.016.

T. Ishlah, “Potensi Bijih besi Indonesia dalam Kerangka Pengembangan Klaster Industri Baja,” Buletin Sumber Daya Geologi, pp. 1–12, 2019.

I. Saefuloh, A. Zahrawani, and B. Adjiantoro, “Pengaruh Proses Quenching Dan Tempering Terhadap Sifat Mekanik Dan Struktur Mikro Baja Karbon Rendah Dengan Paduan Laterit,” J. Tek. Mesin Untirta, vol. IV, no. 1, pp. 56–64, 2018.

M. Y. Hasbi, D. P. Malau, and B. Adjiantoro, “Pengaruh Variasi Reduksi Terhadap Kekerasan dan Struktur Mikro Baja Laterit Melalui Pengerolan Panas,” in Seminar Nasional Sains dan Teknologi, 2016, pp. 1–8.

C. Wen, Y. Tian, G. Wang, J. Hu, and P. Deng, “The Influence of Nickel on Corrosion Behavior of Low Alloy Steel in a Cyclic Wet-dry Condition,” Int. J. Electrochem. Sci., vol. 11, pp. 4161–4173, 2016., doi: 10.20964/110148.

M. Agung Prasetyo, V. Puspasari, M. Syaiful Anwar, A. Nikitasari, and E. Mabruri, “Mechanical properties of modified cast martensitic stainless steel CA6NM with addition of molybdenum and nitrogen,” in AIP Conference Proceeding, 2020, vol. 2232, no. 060001.

I. Díaz et al., “Five-year atmospheric corrosion of Cu , Cr and Ni weathering steels in a wide range of environments,” Corros. Sci., vol. 141, no. July, pp. 146–157, 2018.,

doi: 10.1016/j.corsci.2018.06.039.

S. Herbirowo and B. Adjiantoro, “Pengaruh Perlakuan Panas terhadap Struktur Mikro dan Kekuatan Mekanik Baja Nikel Laterit,” Widyariset, vol. 2, no. 2, pp. 153–160, 2016.

E. Mabruri et al., “Influence of Austenitizing Heat Treatment on the Properties of the Tempered Type 410-1Mo Stainless Steel Influence of Austenitizing Heat Treatment on the Properties of the Tempered Type 410-1Mo Stainless Steel,” IOP Conference Series: Materias Science and Engineering, 2017, doi: 10.1088/1757-899X/202/1/012085.

J. Buckley and B. D. Hansen, “Carburization of Steel Components,” US 10,494,708 B2, 2019.

G. F. Vander Voort, S. R. Lampman, B. R. Sanders, G. J. Anton, C. Polakowski, and M. Park, "ASM Handbook Metallography and Microstructures", vol. 9. Materials Park, Ohio: ASM International, 2004.

G. E. Totten, Steel Heat Treatment Handbook, 2nd Editio. New York: Taylor & Francis Group, 2006.

T. Fras, C. C. Roth, and D. Mohr, “Fracture of high-strength armor steel under impact loading,” Int. J. Impact Eng., vol. 111, pp. 147–164, 2017, doi: 10.1016/j.ijimpeng.2017.09.009.

Y. Takashima, “Fracture toughness evaluation for dissimilar steel joints by Charpy impact test,” Weld. World, vol. 63, pp. 1243–1254, 2019.

G. D. Haryadi, “Pengaruh Suhu Tempering Terhadap Kekerasan, kekuatan Tarik dan Struktur Mikro pada Baja K-460,” ROTASI, vol. 8, no. 2, pp. 1–8, 2014.

W. D. Callister, Fundamental of Materials Science and Engineering, 5th Edition. New York: John Wiley & Sons, Inc., 2001.

A. Azhari, “Pengaruh Proes Tempering dan Proses Pengerolan di Bawah dan di atas Temperatur Rekristalisasi pada Baja Karbon Sedang Terhadap Struktur Mikro untuk Mata Pisau Pemanen Sawit,” J. e-Dinamis, vol. II, no. 2, pp. 10–22, 2012.

G.A. Pantazopoulos, "A Short Review on Fracture Mechanisms of Mechanical Components Operated under Industrial Process Conditions: Fractographic Analysis and Selected Prevention Strategies", Metals, 9, 148, 2019

X. Jin, et.al, " The effect of undissolved and temper-induced (Ti,Mo)C precipitates on hydrogen embrittlement of quenched and tempered Cr-Mo steel", Corrosion Science,https://doi.org/10.1016/j.corsci.2019.108421, 2019




DOI: http://dx.doi.org/10.37209/jtbbt.v10i1.165

Refbacks

  • There are currently no refbacks.


Creative Commons License
This work is licensed under a Creative Commons Attribution-NonCommercial-ShareAlike 4.0 International License.

Address:

Center for Material and Technical Product (B4T)

Jl. Sangkuriang No.14, Bandung, 40135, INDONESIA.

Email : jurnal.tbbt@b4t.go.id

Telp : +62-22-2504088

This work is licensed under a Creative Commons Attribution-NonCommercial-ShareAlike 4.0 International License.

View My Stats